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Grain Size Examination

Grain Size Examination is a metallurgical test used to measure the average size of crystalline grains in a metal or alloy. Grain size plays a key role in determining mechanical properties such as strength, toughness, fatigue resistance, and corrosion performance. For engineered fasteners, controlling grain size is essential to ensuring they perform reliably under demanding conditions.

How the Test is Performed


  1. Sample Preparation – A cross-section of the fastener or material is cut, mounted, and polished to a mirror finish.

  2. Etching – A chemical etchant is applied to reveal grain boundaries in the material.

  3. Microscopic Examination – The prepared sample is examined under an optical microscope.

  4. Measurement – Grain size is determined using comparison charts, line intercept methods, or digital image analysis in accordance with industry standards.

  5. Documentation – Results are recorded and compared against specification requirements.



Why It is Performed


Grain Size Examination is performed to confirm that the material’s microstructure supports the required mechanical properties.

  • Finer grains generally increase strength and toughness (Hall-Petch relationship)

  • Coarser grains may improve high-temperature performance in certain alloys

  • Verifies that heat treatment and forging processes were properly executed

  • Ensures consistency and reliability across production batches

Application to Engineered Fasteners


Engineered fasteners are used in critical applications where mechanical performance and reliability are non-negotiable. Grain size testing ensures that:

  • Heat-treated fasteners achieve the desired strength and fatigue resistance

  • Forged components exhibit proper grain flow and uniformity

  • Material properties remain consistent across production lots

  • Industry-specific performance requirements are met for sectors such as aerospace, nuclear, oil & gas, and defense



Standards & Compliance


TSP Manufacturing performs Grain Size Examinations in accordance with ASTM E112, ISO 643, and customer-specific requirements. Our trained metallurgical team uses calibrated equipment and standardized methods to deliver accurate, repeatable, and traceable results. By adhering to these rigorous standards, TSP demonstrates its commitment to producing engineered fasteners and machined components with verified structural integrity and long-term reliability.

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